SYNTHESIS OF Fe3BO6 NANOPARTICLES BY CHEMICAL DEPOSITION TO OBTAIN Nd-Fe-B MAGNETICALLY HARD ALLOY

Authors

Odilzhon ABDURAKHMONOV, Tashkent Chemical-Technological Institute, Tashkent, UzbekistanFollow
Marat ALISULTANOV, University of Chemical Technology of Russia, Moscow, RussiaFollow
Sherzod ABDURAKHMONOV, Almalyk branch of the National Research Technological University "MISiS", Almalyk, UzbekistanFollow
Aytan MURADOVA, University of Chemical Technology of Russia, Moscow, RussiaFollow

DOI

10.34920/cce202313

Abstract

The purpose of this work is the synthesis of Fe3BO6 nanoparticles for use as the main component in the chemical method for obtaining nanostructured Nd-Fe-B alloys. Amorphous Fe3BO6 nanoparticles prepared by chemical precipitation, FeCl3, and NaBH4 precipitant were used as precursors. Thermal treatment yielded Fe3BO6 crystalline nanoparticles. To determine the thermal effects and phase transitions were carried out: thermogravimetric analysis, differential scanning calorimetry (TG-DSC) and X-ray phase analysis (XRF). The morphology of the obtained nanoparticles was studied using scanning and transmission electron microscopy (SEM and TEM). It has been established that at a temperature of 530 °C, the complete formation of Fe3BO6∙3α-Fe2O3 occurs. The shape of the resulting Fe3BO6∙3α-Fe2O3 particles is incorrect, the average diameter of the nanoparticles was 50±10 nm.

Recommended Citation

ABDURAKHMONOV, Odilzhon; ALISULTANOV, Marat; ABDURAKHMONOV, Sherzod; and MURADOVA, Aytan (2024) "SYNTHESIS OF Fe3BO6 NANOPARTICLES BY CHEMICAL DEPOSITION TO OBTAIN Nd-Fe-B MAGNETICALLY HARD ALLOY," CHEMISTRY AND CHEMICAL ENGINEERING: Vol. 2023: No. 1, Article 3.
DOI: 10.34920/cce202313
Available at: https://cce.researchcommons.org/journal/vol2023/iss1/3